Carburization and Characterization of High-Speed Steel Single-Point Cutting Tools Using Walnut Shell As A Carburizing Agent

Carburization and Characterization of High-Speed Steel Single-Point Cutting Tools Using Walnut Shell As A Carburizing Agent

Authors

  • Tobi Omole Federal University of Technology, Akure (FUTA)

DOI:

https://doi.org/10.51459/jostir.2026.2.2.0110

Abstract

High-speed steel (HSS) cutting tools are essential in modern machining due to their hardness, toughness, and wear resistance. However, tool wear reduces efficiency and increases costs. This study investigates the carburization of M2 HSS single-point cutting tools using walnut shell as a sustainable carbon source. Nine samples were carburized at 850 °C, 900 °C, and 950 °C for holding times of 30, 60, and 90 minutes in a muffle furnace. Post-carburization characterization was conducted using Rockwell hardness testing, scanning electron microscopy (SEM), and energy-dispersive spectroscopy (EDS). Results showed significant hardness enhancement, with the best hardness result at 87.6 HRC60kg, achieved at 950 °C for 90 minutes. SEM revealed refined carbide precipitation, while EDS confirmed increased carbon content on the carburized surfaces microstructure. The study demonstrates that walnut shell is an effective and eco-friendly carburizing medium, providing an economical and sustainable alternative for surface hardening of HSS cutting tools.

Keywords: High-speed steel, Carburization, Walnut shell, Hardness, SEM, Sustainable materials.

References

Adi, S. S., and Malik, V. R. (2025). Friction stir processing of aluminum machining waste: carbon nanostructure reinforcements for enhanced composite performance-a comprehensive review. Materials and Manufacturing Processes 40(3): 285-334.

Afolalu, S., Adejuyigbe, S. B., and Adetunji, O. R. (2015). Impacts of carburizing temperature and holding time on wear of high speed steel cutting tools. International Journal of Scientific and Engineering Research, 6(5), 905-909.

Afolalu, S. A., Salawu, E. Y., Okokpujie, I. P., Abioye, A. A., Abioye, O. P., Udo, M. O., Adetunji, O. R., and Ikumapayi, O. M. (2017). Experimental Analysis of the Wear Properties of Carburized HSS (ASTM A600) Cutting Tool. International Journal of Applied Engineering Research, 12(19), 8995-9003.

Al-Samarai, R. A., and Al-Douri, Y. (2024). Friction and Wear in Metals, Springer.

Aramide, F. O., Ibitoye, S. A., Oladele, I. O., and Borode J. O. (2009). Effects of carburization time and temperature on the mechanical properties of carburized mild steel, using activated carbon as carburizer. scimago Institutions Rankings, 12(4). https://doi.org/10.1590/S1516-14392009000400018.

Duan, H., Han, Y., Lü, W., Mao, J., Wang, L., and Zhang, D. (2016). Effect of solid carburization on surface microstructure and hardness of Ti-6Al-4V alloy and (TiB+La2O3)/Ti-6Al-4V composite. Transactions of Nonferrous Metals Society of China, 26(7), 1871–1877. doi:10.1016/s1003-6326(16)64301-7.

Edun, B. M., Ajayi, O. O., Afolalu, S., Kayode, J. F., Ogundipe, A. T., and Fajugbagbe, A. A. (2024). Utilization of agro-waste materials as viable strengthening agents in carburisation. In Proceedings of the 2024 International Conference on Science, Engineering and Business for Driving Sustainable Development Goals (SEB4SDG). IEEE. https://doi.org/10.1109/SEB4SDG.2024.00

Ehi-Okoebor, C., Salawu, E. Y., Afolalu, S. A., Ajayi, O. O., Kayode, J. F., and Lawal, S. L. (2023). Importance of hybrid organic carburizers on the mechanical properties of mild steel: A review. In Proceedings of the 2023 International Conference on Science, Engineering and Business for Sustainable Development Goals (SEB-SDG). IEEE. https://doi.org/10.1109/SEB-SDG57117.2023.10124621

Elmi Hosseini, S. R., and Li, Z. (2016). Pack Carburizing: Characteristics, Microstructure, and Modeling. Encyclopedia of Iron, Steel, and Their Alloys, 1–24. doi:10.1081/e-eisa-120051080

Kieush, L., Rieger, J., Schenk, J., Brondi, C., Rovelli, D., Echterhof, T., Cirilli, F., Thaler, C., Jaeger, N., Snaet, D., Peters, K., and Colla, V. (2022). A comprehensive review of secondary carbon bio-carriers for application in metallurgical processes: Utilization of torrefied biomass in steel production. Metals, 12(12), 2005. https://doi.org/10.3390/met12122005

M'Saoubi, R., Outeiro, J.C., Chandrasekaran, H., Dillon Jr., O.W., and Jawahir, I.S. (2008). A review of surface integrity in machining and its impact on functional performance and life of machined products. International Journal of Sustainable Manufacturing, 1(1-2), 203-236. https://doi.org/10.1504/IJSM.2008.019234

Oyetunji, A., and Adeosun, S. O. (2012). Effects of Carburizing Process Variables on Mechanical and Chemical Properties of Carburized Mild Steel. Journal of Basic and Applied Sciences, 8, 2-6.

Pupan, L., and Dolya, V. (2022). Basics of Cutting Theory and Cutting Tools.

Sajdak, M., Muzyka, R., Gałko, G., Ksepko, E., Zajemska, M., Sobek, S., and Tercki, D. (2023). Actual trends in the usability of biochar as a high-value product of biomass obtained through pyrolysis. Energies, 16(1), 355. https://doi.org/10.3390/en16010355

Downloads

Published

2026-08-28

How to Cite

Omole, T. (2026). Carburization and Characterization of High-Speed Steel Single-Point Cutting Tools Using Walnut Shell As A Carburizing Agent. Journal of Science, Technology and Innovation Research, 2(2). https://doi.org/10.51459/jostir.2026.2.2.0110

Issue

Section

Articles
Loading...